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Denrées alimentaires liquides, faible viscosité
Échantillonnage

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Denrées alimentaires liquides, faible viscosité
Définition

(liste des codes SH couverts par la présente fiche)		 Low viscosity liquid foodstuffs in bulk, such as beverages, spirits, wine, ketchup, molasses, mustard, soya sauce, sugar syrup, vegetable oils, vinegar, and water. Les marchandises mentionnées ci-dessus peuvent également être considérées comme de haute viscosité, suivant leur nature exacte et/ou leur température.

This card also covers animal feed products, liquid, low viscosity.

For frozen products see chapter «Sampling procedures».

Pour les denrées alimentaires liquides de haute viscosité, consultez «Denrées alimentaires liquides, haute viscosité».

Pour les produits conditionnés en emballages individuels, consultez la fiche «Emballages de détail».

Pour les produits laitiers tels que le lait, consultez la fiche dédiée «Produits laitiers».


Denrées alimentaires liquides, faible viscosité
Quantité minimale recommandée pour chaque échantillon 0,5 litre ou 0,5 kg
Normes (ISO et UE) applicables et législation en vigueur
  • EN ISO 707 Milk and milk products — Guidance on sampling.
  • EN ISO 5555 Corps gras d’origines animale et végétale - Échantillonnage
  • Règlement (CE) n° 1989/2003 de la Commission modifiant le règlement (CEE) n° 2568/91 relatif aux caractéristiques des huiles d’olive et des huiles de grignons d’olive ainsi qu’aux méthodes d’analyse y afférentes
  • Commission Implementing Regulation (EU) No 1348/2013 of 16 December 2013 amending Regulation (EEC) No 2568/91 on the characteristics of olive oil and olive-residue oil and on the relevant methods of analysis.
  • Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods of sampling and analysis for the official control of feed.
Veuillez également vous reporter à la législation en vigueur dans votre pays, ainsi qu’à vos lignes directrices nationales en matière d’échantillonnage.


Équipement requis
Outil d’échantillonnage proposé selon la méthode utilisée
  • Pompe à vide (L01-01)
  • Récipient plongeur de divers types et conceptions (L02-01, L02-02)
  • Appareil d’échantillonnage de type pipette (L03-01)
  • Pelle d’échantillonnage (L04-01)
  • Appareil d’échantillonnage à piston (L05-01)
Copper and copper alloys (e.g. brass) must not be used.

Récipients à utiliser pour l’échantillonnage
  • Flacons en verre (G01)
  • Flacons en plastique, à col étroit, contenance de 500 à 1000 ml (P01); idéalement non transparents
  • Récipients métalliques (M01)
Tous les récipients doivent être adaptés aux denrées alimentaires, et notamment aux produits très acides.

Mesures de précaution et évaluation des risques
  • You should be aware of and follow any health and safety instructions in the local risk assessment and/or safe working practices for the location where the sampling is to take place.
  • Pay attention to any safety labels.
  • If you have indications that there are dangerous goods, request the SDS or ADR.
  • See Health and Safety for the ‘Sampling of Food Products’ for detailed advice on hygiene and risks for liquid products.
  • The hygiene of food products must be maintained.
  • Ensure you have clean and appropriate PPE for the circumstances.
  • Flammable liquids such as ethanol create a risk of fire, particularly when the product is moved. Ensure there is no accumulation of static electricity, be aware of flammable vapours. See Health and Safety.

Plan d’échantillonnage
Type d’envoi Procédure
Envoi à dédouaner One aggregate sample consists of an appropriate number of incremental samples chosen randomly or systematically throughout the consignment. When you are satisfied the consignment is homogeneous, one incremental sample is usually taken as representing the goods covered by the same customs declaration.
Lots PAC (restitutions à l’exportation) ou contrôle d’accises L’échantillon global se compose d’un nombre approprié d’échantillons élémentaires. Le nombre minimal d’échantillons élémentaires est décrit ci-dessous. Si l’envoi se compose de marchandises en provenance d’une seule et même ligne de production (numéro de lot identique), un nombre réduit d’échantillons peut être prélevé.
Citernes verticales fixes, citernes horizontales fixes, navires-citernes, wagons-citernes ou camions-citernes One aggregate sample from one or more incremental samples taken from different heights depending on the liquid level in the tank and number of tanks chosen randomly or systematically throughout the consignment, see Sampling of liquids, ‘1.1 Sampling from tanks and 1.2 Sampling from ships or barges‘ in the General part.

Check the homogeneity of the lot — if the homogeneity is in doubt, take more incremental samples. More aggregate samples should be created from tanks if containing different products or lots.

An aggregate sample is prepared from incremental samples taken from the same tank. If an aggregate sample is for multiple tanks, it must consist of proportional parts from each tank sampled.

The sample is usually taken from top openings through the hatch or by means of special sampling taps placed at the side of tanks at the correct heights. Cross-sectional sampling can be also used. A vacuum pump may also be used if the depth from which the sample is to be taken does not exceed 4 m.

Samples can be also taken during loading or discharging as the liquid is being moved.
Transport packages, barrels, drums, cases, tins One or more aggregate samples: from incremental samples (one or more depending on the product homogeneity, number of containers) drawn from the middle of each container chosen randomly or systematically throughout the consignment, see Sampling of liquids, ‘1.3 Sampling from barrels, cans, tins and other transport packages‘ in the General part.

An aggregate sample may be formed only from containers from the same lot contained in the same consignment. If there are several lots, they should be identified and sampled separately.

If possible, properly homogenize the content of the container before sampling.

The sampling is performed by using a vacuum pump, various pipette-type samplers or other appropriate samplers.

If a sample is taken from only one container (e.g. barrel), it is poured directly from the sampler into the sample container.
Denrées alimentaires liquides en mouvement One aggregate sample: Where the product is being mechanically moved by gravity, pumps or other equipment, there may be diverter valves at the side of fuel line that allow samples to be drawn at regular intervals determined by the moving speed from the fuel stream, see Sampling of liquids, ‘1.6 Sampling from moving cargo‘ in the General part.

Manipulation des échantillons
Commentaires généraux
  • Si le produit est transporté en vrac non emballé, le chargement doit être considéré comme un tout, et les échantillons doivent être prélevés dans toutes les parties de celui-ci.
  • Continuous automatic sampling is always the preferred method as opposed to manual sampling.
  • Determine whether there is sediment or an emulsion layer or free water at the bottom of the tank by means of a bottom sampler and/or water detectors. It is desirable, as far as possible, to run off free water before sampling, and to measure the amount removed.
  • When possible, take a running sample directly into the sample bottle. This reduces the possibility of air absorption, loss of vapours, and contamination. Just before sampling, rinse the bottle with the product to be sampled. Use pre-cooled bottles in summer months for volatiles (e.g. for ethanol).
  • If a mixing vessel is used, it must be pre-washed with the sampled product. All incremental samples from all sampling spots are collected and after they have been thoroughly mixed, an aggregate sample is created. Use a pre-cooled mixing vessel in summer months for volatiles (e.g. for ethanol).
  • The container should be filled to a maximum of 90 % of its volume, to allow expansion due to heat and then sealed to prevent the loss of moisture. It should be kept out of direct sunlight.
Formulaire d’échantillonnage
  • Remplissez le formulaire d’échantillonnage. Un exemplaire de celui-ci doit être joint aux échantillons et un autre conservé pour référence.
Transport
  • The samples must be protected against light and odour to prevent contamination, microbiological growth or other situations which would damage the sample.
  • If necessary keep cooled. The cooling chain must be maintained and should be recorded.
  • Flammable liquids are a hazardous material the transport of which is governed by ADR rules. Exemptions for dangerous goods packed in limited quantities can be applied. When combination packages are used (consisting of an inner and an outer packaging not liable to break or be easily punctured), it is permitted to transport a maximum of 30 l, of which a maximum of 10 l may be class 1 flammable products e.g. ethanol, see Transport in the General part.
Stockage
  • Protect the samples from sources of contamination (odour, liquids, etc.) and contact with other substances.
  • For perishable goods:
    • Keep cooled or refrigerated below 4 °C. The temperature of the cooling chain should be recorded.
    • For longer storage freeze the samples at -18 °C or lower and monitor the temperature during storage.

Denrées alimentaires liquides, faible viscosité (Développer la liste)
Code SH Description


Révisions
Version Date Modifications
1.0 12.10.2012 Première version
1.1 15.01.2021 New format, addition of animal feed HS Codes and other modifications